Cholesterol Staining

Hi,

Can someone help me with the protocol for the choleterol staining using filipin (which’s a fluroscent antibiotic from sigma). I have been trying it for quite some time now but doesn’t seem to work.

Please specify the excitation - emission wavelengths.

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Hi Lee

Filipin is a fluorescent polyene antibiotic commonly used to stain unesterified cholesterol in cell membranes. So if your cholesterol is esterified, it will not work.

A generalized protocol may be used as below

  1. Fix Cells: Wash the cells with PBS twice to remove any media.
  2. Fix the cells with 4% paraformaldehyde in PBS for 15-20 minutes at room temperature.
  3. Wash the cells three times with PBS to remove residual fixative.

3. Filipin Staining

  1. Prepare Filipin Solution: Dissolve Filipin complex in PBS or DMSO to a final concentration of 50-200 µg/mL. Use freshly prepared or store aliquots at -20°C for up to a week to avoid degradation.
  2. Stain Cells: Incubate the fixed cells with the Filipin solution for 30-60 minutes at room temperature in the dark (Filipin is light-sensitive).
  3. Wash Cells: After staining, wash the cells three times with PBS to remove excess dye.

4. Imaging

  1. Mount Coverslips: Mount the coverslips on glass slides using an appropriate mounting medium that preserves fluorescence.
  2. Fluorescence Microscopy:
  • Excitation Wavelength: 340-380 nm (UV range)
  • Emission Wavelength: 430-475 nm (blue fluorescence)
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